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◆ The Review of scientific instruments2026-09-01

A high field magnetic force microscope for imaging air-sensitive materials.

Aile Wang, Shuai Dong, Kesen Zhao, Junwei Liu, Ze Wang, Min Zhang, Jihao Wang, Jing Zhang, Qiyuan Feng, Yubin Hou, Yalin Lu, Wenjie Meng, Qingyou Lu

原始摘要(英文原文)· Original abstract
Imaging measurements of the intrinsic magnetic structures of air-sensitive materials have long posed significant technical challenges. Here, we present a novel magnetic force microscope (MFM) scanning head design that incorporates a rubber O-ring and a threaded sealing assembly to achieve independent, airtight encapsulation of the sample. The fully assembled scanning head exhibits a compact form factor, with an outer diameter of only 24 mm and a total length of merely 80 mm. Based on this design, we have constructed a MFM system tailored for imaging magnetic structures in air-sensitive materials. This MFM system enables operation at magnetic fields of up to 11.7 T and temperatures as low as 5 K. Using this system, we have successfully visualized the evolution of intrinsic magnetic domains in the air-sensitive material VI3 as a function of temperature and applied magnetic field at 5 K. In addition, twin domains arising from structural phase transitions are clearly resolved. Owing to its compact dimensions and high compatibility, the proposed MFM scanning head holds considerable potential for integration into higher-field setups, such as water-cooled bitter magnets, opening avenues for exploring magnetic structures of air-sensitive quantum materials under previously inaccessible experimental regimes.
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A high field magnetic force microscope for imaging air-sensitive materials. — 科研速览 Science Skim