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◆ Organic letters2026-08-14

Stereospecific Strain-Release-Driven Ring Opening of Azabicyclo[1.1.0]butanes to Access N-β-Substituted Chiral Azetidines.

Debraj Ghorai, Arpan Naskar, Rupam Sahoo, Santanu Panda

原始摘要(英文原文)· Original abstract
Chiral azetidines bearing stereocenters remote from the azetidine ring represent highly valuable and structurally diverse motifs that are frequently encountered in a variety of bioactive compounds. Over the past few years, several catalytic ring-opening strategies involving azabicyclo[1.1.0]butanes (ABBs) have been developed for the synthesis of functionalized azetidines. However, the efficient synthesis of azetidines containing well-defined chiral centers remains a significant challenge. Herein, we report a dual strain-release ring-opening reaction of ABB carbinols with aziridines, merging two strained rings, enabling the synthesis of enantiopure N-β-amino-C3-quaternary chiral azetidines.
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Stereospecific Strain-Release-Driven Ring Opening of Azabicyclo[1.1.0]butanes to Access N-β-Substituted Chiral Azetidines. — 科研速览 Science Skim