Cuong Nguyen, Yingang Liu, Anh Kiet Tieu, Haiwei Chang, Xuan Vu Nguyen, Guanyu Deng, Mingxing Zhang, Huijun Li, Lihong Su
In this study, AlCrFeNiMo high-entropy alloy (HEA) coatings have been successfully fabricated by laser cladding method using the mixed elemental powders as the raw material. Two different laser powers (200 W for HEA1 and 350 W for HEA2) were used, aiming to investigate the influence of processing parameters on the phase constitution, microstructure and properties of as-cladded HEA coatings. It has been found that both AlCrFeNiMo HEA coating is consisted of BCC1, BCC2 and Mo-rich phases. HEA2 exhibited finer microstructure, reduced elemental segregation, and slightly higher hardness (833.3 HV) compared to HEA1 (808.6 HV). Tribological testing from room temperature to 900 °C showed that HEA2 consistently achieved lower friction coefficients and wear rates with lowest values of 0.29 and 0.68 × 10 −5 mm 3 /Nm at 900 °C, respectively. Cross-sectional and surface analyses revealed a transition from abrasive wear at room temperature to oxidative wear at 900 °C, with HEA2 forming a denser, stable tribo-oxide layer enriched in Al and Cr. These results highlight that optimizing laser processing enhances the microstructural integrity and high-temperature wear resistance of AlCrFeNiMo HEA coatings, making them promising for extreme service conditions.